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Table 4 Mean contents and proposed content limits for kukoamines A and B in Lycii Cortex

From: Quality control of Lycium chinense and Lycium barbarum cortex (Digupi) by HPLC using kukoamines as markers

Parameters

KA

KB

Caa

3.49

10.75

SDb

2.51

6.31

RSDc

71.91

58.73

nd

16

t ecritical

2.131

uc (C)f

0.46

2.67

Calculated limitg

1.45

4.72

Outlierh

0

0

Failing rate (%)i

12.50

18.75

  1. aCa, average content of klkukoamines in samples (mg/g)
  2. bSD, standard deviation of the contents in all samples
  3. cRSD (%) = 100 × SD/mean
  4. dn, sample size
  5. etcritical, critical value for a 95% confidence interval when the sample size was 16
  6. f uc (C), combined standard uncertainty of the kukoamine B content in the sample (mg/g). The calculation is shown in the supplementary data section
  7. gCalculated limit for kukoamines in the sample. The calculation is shown in the supplementary data section
  8. hNumber of outlier samples. The data are referenced to Table 1
  9. iPercentage of samples with kukoamine contents outside the calculated limits