Fig. 1

Optimization of SPME conditions. a SPME fiber (1, 65 μm PDMS/DVB; 2, 100 μm PDMS; 3, 85 μm Polyacrylate; 4, 75 μm CAR/PDMS). b Extraction temperature. c Extraction time. d Particle sizes. All data was presented as average of two determinations, their relative average deviations were less than 4.7%